NTP CHEMICAL REPOSITORY (RADIAN CORPORATION, AUGUST 29, 1991)

MALONONITRILE




IDENTIFIERS





CATALOG ID NUMBER: 001212

CAS NUMBER: 109-77-3

BASE CHEMICAL NAME: MALONONITRILE

PRIMARY NAME: MALONONITRILE

CHEMICAL FORMULA: C3H2N2

STRUCTURAL FORMULA:

WLN: NC1CN

SYNONYMS:
CYANOACETONITRILE
DICYANOMETHANE
MALONIC DINITRILE
METHANE, DICYANO
USAF A-4600
METHANE CYANINE





PHYSICAL CHEMICAL DATA






PHYSICAL DESCRIPTIONS: Brown solid

MOLECULAR WEIGHT: 66.06

SPECIFIC GRAVITY: 1.1910 @ 20/4

DENSITY:Not available

MP (DEG C): 32 C ( also given as 30.0-30.5 C)

BP (DEG C): 218-219 C degrees at 760 mm Hg

SOLUBILITIES:
WATER : >=100 mg/mL @ 22.5 C (RAD)

DMSO : >=100 mg/mL @ 22.5 C (RAD)

95% ETHANOL : >=100 mg/mL @ 22.5 C (RAD)

METHANOL : Not available

ACETONE : >=100 mg/mL @ 22.5 C (RAD)

TOLUENE : Not available

OTHER SOLVENTS:
Water:soluble
Alcohol:very soluble
Chloroform:soluble
Acetic Acid:soluble
ETHER : Very soluble
BENZENE: soluble

VOLATILITY : Not available

FLAMMABILITY(FLASH POINT):
The flash point for this compound is 112 C (459 F), and it is combustible.
Fires involving this compound can be controlled using dry chemical, carbon
dioxide or Halon extinguishers.

UEL: Not available LEL: Not available

REACTIVITY: This compound may polymerize violently on heating or with strong b

STABILITY: This compound is sensitive to prolonged exposure to air.

OTHER PHYSICAL DATA: Refractive index:1.4146 @ 34 C degrees





TOXICITY






NIOSH REGISTRY NUMBER: OO3150000

TOXICITY:

  typ. dose       mode     specie     amount       unit      other

       LD50        orl        rat         61      mg/kg

       LDLo        ink        rat          7      mg/kg

       LD50        orl        mus         19      mg/kg

       LD50        ipr        mus         13      mg/kg

       LD50        ivn        mus         32      mg/kg

       LDLo        unk        mus          8      mg/kg



AQTX/TLM96: Not available

SAX TOXICITY EVALUATION: THR: High via ip.,oral,and inhalation routes

CARCINOGENICITY: Not available

MUTAGENICITY: Not available

TERATOGENICITY: Not available

STANDARDS, REGULATIONS & RECOMMENDATIONS:
OSHA: None
ACGIH: None
NIOSH Criteria Document: Recommended Exposure Limit to this compound-air:
TWA 3 ppm [610]
NFPA Hazard Rating: Health (H): None
Flammability (F): None
Reactivity (R): None

OTHER TOXICITY DATA:
Skin and Eye Irritation Data:
eye-rbt 5 mg/24H SEV
Status: Reported in EPA TSCA Inventory, 1980
Meets criteria for proposed OSHA Medical Records Rule





OTHER DATA (Regulatory)





PROPER SHIPPING NAME (IATA): Malononitrile

UN/ID NUMBER: UN2647

HAZARD CLASS: 6.1 SUBSIDIARY RISK: None PACKING GROUP: II

LABELS REQUIRED: Poison

PACKAGING: PASSENGER: PKG. INSTR.: 613, Y613 MAXIMUM QUANTITY: 25 kg, 1 kg
CARGO : PKG. INSTR.: 615 MAXIMUM QUANTITY: 100 kg

SPECIAL PROVISIONS: None

USES: Organic synthesis; leaching agent for gold.

COMMENTS: Not available





HANDLING PROCEDURES






ACUTE/CHRONIC HAZARDS:
This compound is readily absorbed through the skin.

MINIMUM PROTECTIVE CLOTHING:
If Tyvek-type disposable protective clothing is not worn during
handling of this chemical, wear disposable Tyvek-type sleeves taped to
your gloves.

RECOMMENDED GLOVE MATERIALS: Not available

RECOMMENDED RESPIRATOR:
Where the neat test chemical is weighed and diluted, wear a NIOSH-
approved half face respirator equipped with a combination filter cartridge,
i.e. organic vapor/acid gas/HEPA (specific for organic vapors, HCl, acid
gas, SO2 and a high efficiency particulate filter).

OTHER: Not available

STORAGE PRECAUTIONS:
You should keep this material in a tightly-closed container
under an inert atmosphere, and store it at refrigerated temperatures.

SPILLS AND LEAKAGE:
If you spill this chemical, you should dampen the solid spill material
with water,then transfer the dampened material to a suitable container. Use
absorbent paper dampened with water to pick up any remaining material. Seal
your contaminated clothing and the absorbent paper in a vapor-tight plastic
bag for eventual disposal. Wash all contaminated surfaces with a strong soap
and water solution. Do not reenter the contaminated area until the Safety
Officer (or other responsible person) has verified that the area has been
properly cleaned.

DISPOSAL AND WASTE TREATMENT:
You should dispose of all waste and contaminated materials
associated with this chemical as specified by existing local,
state and federal regulations concerning hazardous waste disposal.
It is suggested that your contaminated materials should be destroyed
by incineration in a special, high temperature ( >2000 degrees F),
chemical incinerator facility.





EMERGENCY PROCEDURES






SKIN CONTACT:
IMMEDIATELY flood affected skin with water while removing and isolating
all contaminated clothing. Gently wash all affected skin areas thoroughly
with soap and water.
IMMEDIATELY call a hospital or poison control center even if no symptoms
(such as redness or irritation) develop.
IMMEDIATELY transport the victim to a hospital for treatment after
washing the affected areas.

INHALATION:
IMMEDIATELY leave the contaminated area; take deep breaths of fresh air.
IMMEDIATELY call a physician and be prepared to transport the victim to a
hospital even if no symptoms (such as wheezing, coughing, shortness of breath,
or burning in the mouth, throat, or chest) develop.
Provide proper respiratory protection to rescuers entering an unknown
atmosphere. Whenever possible, Self-Contained Breathing Apparatus (SCBA)
should be used; if not available, use a level of protection greater than or
equal to that advised under Respirator Recommendation.

EYE CONTACT:
First check the victim for contact lenses and remove if present. Flush
victim's eyes with water or normal saline solution for 20 to 30 minutes while
simultaneously calling a hospital or poison control center.
Do not put any ointments, oils, or medication in the victim's eyes without
specific instructions from a physician.
IMMEDIATELY transport the victim after flushing eyes to a hospital even if
no symptoms (such as redness or irritation) develop.

INGESTION:
If the victim is conscious and not convulsing, give 1 or 2 glasses of
water to dilute the chemical and IMMEDIATELY call a hospital or poison control
center.
Generally, the induction of vomiting is NOT recommended outside of a
physician's care due to the risk of aspirating the chemical into the victim's
lungs. However, if the victim is conscious and not convulsing and if medical
help is not readily available, consider the risk of inducing vomiting because
of the high toxicity of the chemical ingested. Ipecac syrup or salt water may
be used in such an emergency. IMMEDIATELY transport the victim to a hospital.
If the victim is convulsing or unconscious, do not give anything by mouth,
ensure that the victim's airway is open and lay the victim on his/her side with
the head lower than the body. DO NOT INDUCE VOMITING. IMMEDIATELY transport
the victim to a hospital.

SYMPTOMS:
Information concerning the symptoms associated with acute exposure to
this compound is not available.

FIREFIGHTING: Not available





SOURCES






SOURCES:
Aldrich Chemical Company. Aldrich Catalog/Handbook of Fine
Chemicals. Aldrich Chemical Co., Inc. Milwaukee, WI.
1980. p.594.

Oak Ridge National Laboratory. Environmental Teratogen Information
Center (ETIC), Bibliographic Data Base. Oak Ridge National
Laboratory. Oak Ridge, TN. Listed.

Oak Ridge National Laboratory. Environmental Mutagen Information
Center (EMIC), Bibliographic Data Base. Oak Ridge National
Laboratory. Oak Ridge, TN. Listed.

U.S. Environmental Protection Agency, Office of Toxic Substances.
Toxic Substances Control Act Chemical Substances Inventory,
Initial Inventory. 6 Vols. U.S. Environmental Protection
Agency. Washington, D.C. 1979. Listed.

Hawley, G.G., Ed. The Condensed Chemical Dictionary. 10th Ed.
Van Nostrand Reinhold. New York. 1981. p.639.

Sax, N.I. Dangerous Properties of Industrial Materials. 5th Ed.
Van Nostrand Reinhold. New York. 1979. p.527.

Buckingham, J., Ed. Dictionary of Organic Compounds. 5th Ed.
Chapman and Hall. New York. 1982. Vol.5, p.4778, P-02348.

Weast, R.C. and M.A. Astle, Eds. CRC Handbook of Chemistry
and Physics. 60th Ed. CRC Press, Inc. Boca Raton, FL.
1982. p.366, m-25.

Lewis, R.J., Sr. and R.L. Tatken, Eds. Registry of Toxic Effects
of Chemical Substances. Microfiche Ed. National Institute for
Occupational Safety and Health. Cincinnati, OH. Quarterly
Updates. OO3150000.

[610] Clansky, Kenneth B., Ed. Suspect Chemicals Sourcebook: A Guide to
Industrial Chemicals Covered Under Major Federal Regulatory and
Advisory Programs. Roytech Publications, Inc. Burlingame, CA.
1990. Update, p. xxix.

[620] United States National Toxicology Program. Chemical Status Report.
NTP Chemtrack System. Research Triangle Park, NC. November 6, 1990.
Not listed.

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